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SCX Chemistry · Chapter 9: Gravimetry, hydrated salts and titrations

Year 11 SCX · About 18 minutes with activities · Turn your sound on

Chapter 9 · Gravimetry and titrations
15.0 g of crystalsnickel sulfate, NiSO₄·6H₂O
Dissolution→Precipitation→Filtration→Washing→Drying to constant mass
Burette0.159 mol L⁻¹ NaOH
25.0 mL H₂SO₄in a conical flask
Pipettedelivers exactly 25.0 mL
Reading: 20.45 mLbottom of the meniscus

Chapter 9 recap

  • Constant mass: heat, cool, weigh, and repeat until the mass no longer changes. Precipitation gravimetry: dissolution → precipitation → filtration → washing → drying to constant mass.
  • Water of crystallisation: the mass lost on heating is water. NiSO₄·6H₂O: 15.0 g → 8.84 g NiSO₄ + 6.16 g H₂O, so 41.1% water.
  • n = cV (V in L); mol L⁻¹ × M = g L⁻¹. Titration: three concordant titres → n = cV → mole ratio → c = n ÷ V. DF = V(flask) ÷ V(pipette).
  • Course complete: revise any chapter from the course home page

How much water hides inside a dry-looking crystal?

Chapter 9 · About 18 minutes · sound on

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